To recover phenolic compounds from olive mill wastewater (a dark, acidic matrix made
up of water, organic substances, including carbohydrates, pectins, mucilage, lignin, and
tannins (which give it a characteristic dark colour), lipids and inorganic substances),
three separation methods (solvent extraction, membrane filtration, and adsorption
utilizing Date palm trunk fiber (DPTF)) were performed. The effects of adsorbent dose,
size, and adsorption period were investigated for the adsorption experiment, whereas
the effects of the extraction time, solvent to water ratio, and feed pressure were
investigated for both the solvent extraction and membrane experiments, respectively.
Four standard solutions of phenol and catechol were prepared to quantify the
concentrations of them using gas chromatography analysis (GC). The results
demonstrate that the fiber was ineffective in recovering catechol and phenol regardless
of the adsorbent dose, size, or even the adsorption period, with nearly 0% recovery,
whereas ethyl acetate and membrane filtration were quite effective in recovering
catechol from OMW, with recovery efficiencies of 80% and 40%, respectively, unlike
hexane, which was also ineffective in the catechol-phenol recovery with almost 0%
recovery.